硅烷化玻璃器皿
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  • 硅烷化玻璃器皿

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Siliconizing GlasswareCaution: Wear gloves and lab coat. Work with dichlorodimethylsilene in hood.
    Fill large dessicator with glassware. Put 1 ml dichlorodimethylsilene in a small beaker and put it in the dessicator. Pull vacuum (water aspirator) for 5 min. Pull off hose to open vacuum quickly and pull vacuum on it for 5 min. Close dessicator and keep under vacuum for 2 hr under hood (turn off water). Remove the glassware from dessicator and bake at least 2 hr at 180 C (375 F).


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