Solvents NMR 位移表及文件
NMR Solvents
| Solvent |
Formula |
1H shifts |
13C shifts |
mp °C |
bp °C |
| Acetic Acid-d4 |
CD3COOD |
2.0, 11.7 |
20.0, 180.0 |
16.6 |
117.9 |
| Acetone-d6 |
CD3COCD3 |
2.09 |
29.9, 206.7 |
-94.7 |
56.1 |
| Acetonitrile-d3 |
CD3CN |
1.94 |
1.4, 118.7 |
-43.8 |
81.6 |
| Benzene-d6 |
C6D6 |
7.16 |
128.4 |
5.5 |
80.1 |
| Carbon Disulphide |
CS2 |
none |
192.8 |
-11.6 |
46.3 |
| Carbon Tetrachloride |
CCl4 |
none |
96.7 |
-23.0 |
76.8 |
| Chloroform-d |
CDCl3 |
7.24 |
77.23 |
-63.5 |
61.3 |
| Dichloromethane-d2 |
CD2Cl2 |
5.32 |
54.0 |
-95.1 |
40.8 |
| Diethyl Ether (-100 °C) |
(CH3CH2)2O |
|
?, 66.51 |
-116.3 |
34.6 |
| Dimethyl Ether (-100 °C) |
CH3OCH3 |
3.2 |
60.08 |
-138.5 |
-23 |
| N,N-Dimethyl formamide-d7 |
Me2NCHO |
2.95, 2.75, 8.03 |
29.8, 34.9, 163.2 |
-61.? |
153.? |
| Dimethyl Sulfoxide-d6 |
CD3SOCD3 |
2.50 |
39.5 |
18.6 |
189.0 |
| 1,4-Dioxan |
(OCH2CH2)2 |
3.53 |
66.7 |
11.8 |
101.4 |
| Ethanol-d6 |
CD3CD2OD |
1.11, 3.56, 5.19 |
17.3, 57.0 |
-117 |
78.3 |
| Methanol-d4 |
CD3OD |
3.31, 4.78 |
49.2 |
-97.8 |
64.6 |
| Nitrobenzene |
C6D5NO2 |
7.5, 7.7, 8.1 |
123, 129, 135 |
5.7 |
210.8 |
| Nitromethane-d3 |
CD3NO2 |
4.3 |
57.3 |
-28.6 |
101.2 |
| Pyridine-d5 |
C5D5N |
7.22, 7.58, 8.74 |
123.9, 135.9, 150.2 |
-41.6 |
115.3 |
| 1,1,2,2-Tetrachloroethane |
CHCl2CHCl2 |
? |
75.5 |
-43.8 |
146.3 |
| Tetrahydrofuran-d8 |
C4D8O |
1.73, 3.58 |
25.4, 67.6 |
-108.5 |
65.4 |
| Tetrahydrofuran -100 °C |
C4H8O |
|
?, 67.96 |
|
|
| Toluene-d8 |
C6D5CD3 |
2.09, 6.98, 7.00, 7.09 |
20.4, 125.5, 128.3, 129.4, 137.9 |
-94.9 |
110.6 |
| Trichlorofluoromethane |
CFCl3 |
none |
117.6 |
-111 |
23.7 |
| Trifluoroacetic Acid-d4 |
CF3COOD |
11.5 |
116.6, 164.2 |
-15.3 |
72.4 |
| Trifluoroethanol-d3 |
CF3CD2OD |
3.88, 5.02 |
61.5, 126.3 |
-15.3 |
72.4 |
| Water |
D2O |
4.8 |
none |
0.0 |
100.0 |
| Solvent |
Formula |
1H shifts |
13C shifts |
mp °C |
bp °C |
Solvent NMR.rar[Download](说明: )
上一篇：TLC和柱层析的关系 下一篇：SynGen (化学反应设计) Solubility Database
|
